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Chemical modification in and on single phase [NiO]0.5[Al2O3]0.5 nanopowders produces “chocolate chip‐like” Nix@[NiO]0.5‐x[Al2O3]0.5 nanocomposite nanopowders

dc.contributor.authorWang, Fei
dc.contributor.authorSun, Kai
dc.contributor.authorYi, Eongyu
dc.contributor.authorLaine, Richard M.
dc.date.accessioned2019-10-30T15:29:51Z
dc.date.availableWITHHELD_15_MONTHS
dc.date.available2019-10-30T15:29:51Z
dc.date.issued2019-12
dc.identifier.citationWang, Fei; Sun, Kai; Yi, Eongyu; Laine, Richard M. (2019). "Chemical modification in and on single phase [NiO]0.5[Al2O3]0.5 nanopowders produces “chocolate chip‐like” Nix@[NiO]0.5‐x[Al2O3]0.5 nanocomposite nanopowders." Journal of the American Ceramic Society 102(12): 7145-7153.
dc.identifier.issn0002-7820
dc.identifier.issn1551-2916
dc.identifier.urihttps://hdl.handle.net/2027.42/151834
dc.description.abstractPhase‐pure [NiO]0.5[Al2O3]0.5 spinel nanoparticles (NPs) with limited aggregation were obtained via liquid‐feed flame spray pyrolysis (LF‐FSP) by combusting metalloorganic precursor solutions. Thereafter “chocolate chip‐like” Nix[NiO0.5‐x][Al2O3]0.5 nanoparticles consisting of primary [NiO0.5‐x][Al2O3]0.5 particles with average particle sizes of 40‐60 nm decorated with Ni metal particles (<10 nm in diameter) dispersed on the surface were synthesized by heat treating the spinel NPs at 800°C/7 h in flowing 5% H2:N2 100 mL/min in a fluidized bed reactor. The synthesized materials were characterized using TEM, XRD, FTIR, and TGA/DTA. The Ni depleted areas consist primarily of γ‐Al2O3. The Ni content (800°C) was determined by TGA to be ≈11.3 wt.% based on TGA oxidation behavior. The successful synthesis of such nanocomposites with limited aggregation on a high temperature support provides a facile route to synthesize well‐defined NP catalysts. This work serves as a baseline study for an accompanying paper, wherein thin, flexible, dense films made from these same NPs are used as regenerable catalysts for carbon nanotube syntheses.
dc.publisherWiley Periodicals, Inc.
dc.subject.otherliquid feed‐flame spray pyrolysis
dc.subject.othernickel aluminate
dc.subject.otherphase pure spinel nanopowders
dc.subject.othernanocomposites
dc.titleChemical modification in and on single phase [NiO]0.5[Al2O3]0.5 nanopowders produces “chocolate chip‐like” Nix@[NiO]0.5‐x[Al2O3]0.5 nanocomposite nanopowders
dc.typeArticle
dc.rights.robotsIndexNoFollow
dc.subject.hlbsecondlevelMaterials Science and Engineering
dc.subject.hlbtoplevelEngineering
dc.description.peerreviewedPeer Reviewed
dc.description.bitstreamurlhttps://deepblue.lib.umich.edu/bitstream/2027.42/151834/1/jace16632_am.pdf
dc.description.bitstreamurlhttps://deepblue.lib.umich.edu/bitstream/2027.42/151834/2/jace16632.pdf
dc.identifier.doi10.1111/jace.16632
dc.identifier.sourceJournal of the American Ceramic Society
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dc.owningcollnameInterdisciplinary and Peer-Reviewed


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