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Synthesis and characterization of cage and bicyclic silsesquioxanes via dehydration of silanols
(John Wiley & Sons, Ltd., 1999-04)
Synthesis of cage and ladder silsesquioxanes by the dehydration of silanols using dicyclohexylcarbodiimide (DCC) is described. The reaction of 1,3-dicyclohexyldisiloxane-1,1,3,3-tetraol with DCC gave octa(cyclohexylsilsesquioxane) ...