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Preparation of 6‐ 3 H glucocerebroside

dc.contributor.authorMcMaster, Marvin C.en_US
dc.contributor.authorRadin, Norman S.en_US
dc.date.accessioned2012-03-16T15:56:55Z
dc.date.available2012-03-16T15:56:55Z
dc.date.issued1977en_US
dc.identifier.citationMcMaster, Marvin C.; Radin, Norman S. (1977). "Preparation of 6‐ 3 H glucocerebroside." Journal of Labelled Compounds and Radiopharmaceuticals 13(3): 353-357. <http://hdl.handle.net/2027.42/90217>en_US
dc.identifier.issn0362-4803en_US
dc.identifier.issn1099-1344en_US
dc.identifier.urihttps://hdl.handle.net/2027.42/90217
dc.description.abstractGlucocerebroside (1–0‐β‐glucosyl ceramide) can be labeled with 3 H‐borohydride at the 6‐position of the glucose moiety. The 6‐trityl ether of cerebroside is formed first, the remaining hydroxyl groups are acetylated, the trityl group is removed, and the free 6‐hydroxyl group is oxidized to an aldehyde. The carbonyl group is then reduced with borohydride and the acetyl groups are removed, regenerating the original glycolipid.en_US
dc.publisherJohn Wiley & Sons, Ltd.en_US
dc.subject.otherAcetate Estersen_US
dc.subject.otherGlucosyl Ceramideen_US
dc.subject.other6‐Trityl Etheren_US
dc.subject.otherGlucosyl Ceramideen_US
dc.subject.otherGlucose Labeleden_US
dc.subject.otherGlucosyl Ceramideen_US
dc.subject.other3 H‐Glucose Labeleden_US
dc.subject.otherGlucocerebrosideen_US
dc.titlePreparation of 6‐ 3 H glucocerebrosideen_US
dc.typeArticleen_US
dc.rights.robotsIndexNoFollowen_US
dc.subject.hlbsecondlevelRadiologyen_US
dc.subject.hlbtoplevelHealth Sciencesen_US
dc.description.peerreviewedPeer Revieweden_US
dc.contributor.affiliationumMental Health Research Institute and Department of Biological Chemistry, University of Michigan, Ann Arbor, MI 48109, U.S.Aen_US
dc.description.bitstreamurlhttp://deepblue.lib.umich.edu/bitstream/2027.42/90217/1/2580130309_ftp.pdf
dc.identifier.doi10.1002/jlcr.2580130309en_US
dc.identifier.sourceJournal of Labelled Compounds and Radiopharmaceuticalsen_US
dc.identifier.citedreferenceBrady R. O., Kanfer J. N., and Shapiro D. ‐ J. Biol. Chem. 240: 39 ( 1965 )en_US
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dc.identifier.citedreferenceButterworth R. and Hanessian S. ‐ Synthesis 1971: 70en_US
dc.identifier.citedreferencePerrin, D. D., Armarego W. L., and Perrin D. R. ‐ Purification of Laboratory Chemicals, Pergamon Press, New York, 1966en_US
dc.identifier.citedreferenceRadin N. S. ‐ J. Lipid Res. 17: 290 ( 1976 )en_US
dc.identifier.citedreferenceIwamori M., Moser H. W., and Kishimoto Y. ‐ J. Lipid Res. 16: 332 ( 1975 )en_US
dc.identifier.citedreferenceBarton N. W. and Rosenberg, A. ‐ J. Biol. Chem. 250: 3966 ( 1975 )en_US
dc.identifier.citedreferenceDi Cesare J. L. and Rapport M. M. ‐ Chem. Physics Lipids 13: 447 ( 1974 )en_US
dc.identifier.citedreferenceErickson J. S. and Radin N. S. ‐ J. Lipid Res. 14: 133 ( 1973 )en_US
dc.owningcollnameInterdisciplinary and Peer-Reviewed


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