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Preparation of small poly(butylene terephthalate) spheres by crystallization from solution

dc.contributor.authorNichols, Mark E.en_US
dc.contributor.authorRobertson, Richard E.en_US
dc.date.accessioned2006-04-28T18:20:29Z
dc.date.available2006-04-28T18:20:29Z
dc.date.issued1994-02en_US
dc.identifier.citationNichols, Mark E.; Robertson, Richard E. (1994)."Preparation of small poly(butylene terephthalate) spheres by crystallization from solution." Journal of Polymer Science Part B: Polymer Physics 32(3): 573-577. <http://hdl.handle.net/2027.42/38866>en_US
dc.identifier.issn0887-6266en_US
dc.identifier.issn1099-0488en_US
dc.identifier.urihttps://hdl.handle.net/2027.42/38866
dc.description.abstractThe crystallization of poly(butylene terephthalate) (PBT) from moderately dilute solutions of PBT in a diglycidyl ether of bisphenol-A epoxy has been investigated. PBT dissolves in this epoxy approximately 35°C below its usual melting temperature of 227°C to form a one-phase solution. Cooling this solution below 165°C leads to rapid crystallization of the PBT. The resulting mixture of liquid epoxy and crystalline PBT has a low viscosity and contains highly birefringent, individual PBT spherulites. The PBT spherulites have a narrow size distribution and a high surface-to-volume ratio. These particles are suggested to arise from a rapid crystallization that follows liquid–liquid phase separation. © 1994 John Wiley & Sons, Inc.en_US
dc.format.extent815941 bytes
dc.format.extent3118 bytes
dc.format.mimetypeapplication/pdf
dc.format.mimetypetext/plain
dc.language.isoen_US
dc.publisherJohn Wiley & Sons, Inc.en_US
dc.subject.otherChemistryen_US
dc.subject.otherPolymer and Materials Scienceen_US
dc.titlePreparation of small poly(butylene terephthalate) spheres by crystallization from solutionen_US
dc.typeArticleen_US
dc.rights.robotsIndexNoFollowen_US
dc.subject.hlbsecondlevelMaterials Science and Engineeringen_US
dc.subject.hlbtoplevelEngineeringen_US
dc.description.peerreviewedPeer Revieweden_US
dc.contributor.affiliationumDepartment of Materials Science and Engineering, University of Michigan, Ann Arbor, Michigan 48109-2136en_US
dc.contributor.affiliationumDepartment of Materials Science and Engineering, University of Michigan, Ann Arbor, Michigan 48109-2136 ; Department of Materials Science and Engineering, University of Michigan, Ann Arbor, Michigan 48109-2136en_US
dc.description.bitstreamurlhttp://deepblue.lib.umich.edu/bitstream/2027.42/38866/1/090320319_ftp.pdfen_US
dc.identifier.doihttp://dx.doi.org/10.1002/polb.1994.090320319en_US
dc.identifier.sourceJournal of Polymer Science Part B: Polymer Physicsen_US
dc.owningcollnameInterdisciplinary and Peer-Reviewed


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